In this video, the tert butyl hypochlorite (t-BuOCl) is prepared using a method from Organic Syntheses (OrgSyn):
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The product yield was about 86%.
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Tert Butyl Hypochlorite Synthesis
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chemistrylaboratoryorganic chemistry laborganic chemistryorganic synthesisorganic reactionacademic experimentmatsynthesisjacsorganic letterschemical societyOrgSynt-BuOCltert butyl hypochloritet-butyl hypochloritetert butanolt-butanolt-buohChlorination agentbleach organic chemistrysodium hypochloriteamber glassorganic synthesesbalalaie labdr balalaiepositive chlorineorganic hypochlorite